Organic Chemistry I Laboratory

SL 287 Syllabus

Bell Tower

Course Description and Prerequisites

Organic Chemistry Lab 1, SL287

1 Credit

Fall 2021

Course Description:

This laboratory course is to be taken concurrently with SC 381 and provides an opportunity to make measurements and observations, critically interpret the collected data, make chemically logical conclusions, and use chemicals in a safe, efficient, and environmentally sustainable manner.

Prerequisites: SL182

Instructor Information

Name: Tamra Shelly
Office P354c
Office Hours: 
Monday: 8:30am-11:00am and 2:303pm-4:0pm 
Tuesday: virtually, by appointment 
Wednesday: 8:00am-10:00am and 1:00pm-2:30pm
Thursday: 1:30pm-2:30pm
Friday by appointment
other times possible by appointment, email, or hangouts

Name Raymond Kennard                                                             

P230B/ kennardr@husson.edu

207-941-7087
Office Hours: Office hours: M 8-8:50, T 12-2:20, W 8-9:50 and F 8-9:50, W 1-1:50 and By appointment Almost Anytime not in Class

Textbook & Required Materials

Green Organic Chemistry (Custom Reprint)

Green Organic Chemistry (Reprint)

ISBN: 9781711453927

Author: Doxsee

Publisher: Cengage Learning

$117.50 at the Husson University Bookstore

 

OR 

Green Organic Chemistry

ISBN: 978-0534388515

Author: Doxee

Publisher: Cengage Learning

Can be ordered online

 

Also need: safety glasses

bound notebook (with carbonless copies) is also required.  There is one in the Bookstore (100 pages) that can be used for both semesters.  This allows you to pass in the copy of prelab and data for lab reports while working on additional lab materials.  A loose-leaf notebook, ring binder, or photocopies will not be acceptable for class.  This notebook will be the only book allowed during the lab.

Course Outcomes

To be successful after graduation in the Sciences requires that the graduates of the programs have competency in a variety of areas.  Through Husson University's program of required, elective, and General Education courses we strive to produce graduates that fulfill these requirements.   

The following is the list of attributes that the Biology-Biochemistry program at Husson requires for its graduates.

Students must: 

    1. Upon successful completion of SL 381/382 the students should be able to:

       

      Student Learning Outcome

      Pre-lab quiz

      Pre-labs

      Post-labs

      Final exam

      Natural product experiment

      In Class observations

       Apply mathematics to solve quantitative chemical problems and evaluate the results of those calculations to make sure they are physically reasonable.

      X

      X

      X

      X

       

       

      Construct correctly balanced chemical equations, differentiating between catalysts, solvents and reactants.

       

      X

       

       

       

       

      Demonstrate mastery of basic organic chemistry laboratory techniques, including distillation, recrystallization, melting point determination, liquid-liquid extraction, gravity and liquid filtration, MS, UV-Vis, IR and NMR spectroscopy, distillation and chromatography. 

       

       

       

       

      X

      X

      Demonstrate the ability to safely and effectively perform synthetic organic reactions, using proper glassware set-up, handling of hazardous chemicals, and following the prescribed experimental procedures

       

       

       

       

      X

      X

      Extract and interpret information from the analytical data and explain the obtained results and any errors encountered.

       

       

      X

       

      X

       

      Demonstrate the ability to maintain a proper laboratory notebook, which includes clear descriptions of original data, observations and experimental procedures.

       

      X

      X

       

      X

      X

      Interpret laboratory results and data correctly and report findings in a scientific notebook using acceptable and appropriate notational and descriptive content that is understandable.  

       

       

      X

       

      X

       

      Apply principles of scientific ethics and academic integrity to their laboratory behavior, assessment and written work.

      X

      X

      X

      X

      X

      X

      Make use of chemical literature as reference material. Be able to read scientific literature to understand equations, reactions and methods and recreate experimental conditions from that literature.

       

       

       

       

      X

       

      Demonstrate safe laboratory practices through the use of safety data sheets (SDS), appropriate personal protective equipment and appropriate handling of all chemicals, including proper disposal of waste.

       

      X

       

       

      X

      X

      Identify the various parts of the experiment that fulfill the green /sustainable mission of the lab.

       

      X

       

      X

       

       

       

Assessment Mapping

udent Learning Outcome

Pre-lab quiz

Pre-labs

Post-labs

Final exam

In Class observations

 Apply mathematics to solve quantitative chemical problems and evaluate the results of those calculations to make sure they are physically reasonable.

X

X

X

X

 

Construct correctly balanced chemical equations, differentiating between catalysts, solvents and reactants.

 

X

 

 

 

Demonstrate mastery of basic organic chemistry laboratory techniques, including distillation, recrystallization, melting point determination, liquid-liquid extraction, gravity and liquid filtration, MS, UV-Vis, IR and NMR spectroscopy, distillation and chromatography. 

 

 

 

 

X

Demonstrate the ability to safely and effectively perform synthetic organic reactions, using proper glassware set-up, handling of hazardous chemicals, and following the prescribed experimental procedures

 

 

 

 

X

Extract and interpret information from the analytical data and explain the obtained results and any errors encountered.

 

 

X

 

 

Demonstrate the ability to maintain a proper laboratory notebook, which includes clear descriptions of original data, observations and experimental procedures.

 

X

X

 

X

Interpret laboratory results and data correctly and report findings in a scientific notebook using acceptable and appropriate notational and descriptive content that is understandable.  

 

 

X

 

 

Apply principles of scientific ethics and academic integrity to their laboratory behavior, assessment and written work.

X

X

X

X

X

Make use of chemical literature as reference material. Be able to read scientific literature to understand equations, reactions and methods and recreate experimental conditions from that literature.

 

 

 

 

 

Demonstrate safe laboratory practices through the use of safety data sheets (SDS), appropriate personal protective equipment and appropriate handling of all chemicals, including proper disposal of waste.

 

X

 

 

X

Identify the various parts of the experiment that fulfill the green /sustainable mission of the lab.

 

X

 

X

 

Evaluation and Grading

Grading:   Completed IR and NMR spectrum packets and Post-Lab reports (40%) written in the notebook and the copy passed in the next class after completing the lab, Pre-lab reports, (30%) written in the lab notebook and the copy turned in prior to beginning the experiment, Pre-lab quizzes (online, covering concepts, readings and techniques) to be completed before the first day of an experiment (10%),  and a comprehensive final exam, given through ExamSoft and covering all material assigned or covered in lab, given during the last scheduled lab section (20%) form the basis for the determination of final grade.

Computer requirements for ExamSoft.pdf  download

Late assignments will be docked 10% for the first week and will be docked 10% for each week late after that.  Any assignments not passed in will automatically receive a grade of zero

Lab reports are due for each experiment and are divided into two parts, the prelab, due the beginning of class the first day of the experiment, and postlab, due one week after completion of the experiment .

 

The Pre-lab reports MUST be clearly organized and consist of:  

  1. Title and names of lab partners
  2. Purpose – short explanation of what the purpose of the experiment is. For full credit it MUST Include all of the following:
    1. what concepts the experiment is demonstrating,
    2. what techniques are used; and
    3. specifically how this experiment is greener then previous methods. (3 points)
  3. Balanced chemical equation(s) – not mechanism! (2 points). Compounds must be drawn out, no chemical formulas.
  4. Summary of any significant health and safety issues from Section 2 of the SDS for EVERY chemical used in the experiment (0.5 point for each chemical).  Water may be omitted.  For credit, you MUST include the signal words and either the pictogram or Hazard classification in your description.
  5. Personal protective equipment needed for the lab (1 point).
  6. A short description of the techniques needed for the lab, including how to set them up and what their functions are. (0.5 point for each technique)
  7. A short handwritten synopsis of the procedure (2 points)
  8. Answers to any Pre-Lab questions, either in lab book or on Canvas on the reading assignment in Bruice or in the module. (1 point for each question)
  9. Neatness and Organization (1 point)

The Post-lab Reports MUST be clearly organized and contain the following sections:   

 Title and lab partners names

  1. separate discussion of the data/results obtained and an explanation of the results, including error analysis to explain low or high yields. This should be a separate labeled section of the postlab and may include material discussed in post lab questions (4 points).  
  2.  Required calculations: (1 pt each)
    1. limiting reagent
    2. theoretical and percent yields
    3. atom economies
    4. cost analysis for the experiment
  3. Illustrations or print-outs of lab data, including, but not limited to;  IRs, NMRs, TLCs or columns (2 pts each)
  4. Answers to post-lab questions in your book or posted on Canvas not covered in Questions 1,2 or 3 above.(1 point each)

 Organization and neatness (2 points)

 All assignments must be written legibly (if I cannot read the carbon you pass in you do not get credit).  

Assignments will be docked 10% for every week late. 

I try to have all assignments graded and comments back to the students within 3-7 days of the due date.  

Zoom Proctoring

In the event that faculty utilize remote proctoring as a tool to monitor the use of remote exams, proctoring via Zoom is an option. 

  • A laptop capable of supporting Canvas, Examplify, and Zoom
  • A second device that is capable of supporting both video and audio Zoom meetings for remote proctoring
  • Suitable Internet connection to facilitate and sustain video and audio Zoom meetings

 

Canvas Information

Canvas is the where course content, grades, and communication will reside for this course.

Grading Rubrics

N/A

Class Policies

Links to University Policies and student protections as well as student services can be found on the left navigation panel. You can also find a link to information about how to navigate Canvas.

This class is designed to be something worked on with some flexibility with firm due dates. It is important to stay on track and adhere to those. We will need you to complete your materials by that time. If you cannot, then you will need to repeat the course.

You are expected to be in class to participate. If you miss more than one lab period, you will be considered out of compliance with Husson University's attendance requirement.

Instructors Discretion to Modify the Syllabus

The instructor has the authority to modify the syllabus based on (her/his) determination that such changes would better meet the learning objectives of the course.  It is the responsibility of the student to maintain awareness of those modifications and note them as necessary.  The instructor also has full discretion to determine the extent to which (if at all) technology will be used and/or available within the classroom.  Such determination could be based on technology as a learning tool or simply to minimize distractions among students.  

As most students here at Husson are in pre-professional programs we expect proper behavior, courtesy, and respect for all individuals in a class.  All University policies will be strictly adhered to in class.

We will meet the first week of classes and you must be properly attired for lab on that day.  Proper attire is ALWAYS required in lab, regardless of the experiment!  Closed-toed shoes, long hair tied back and long skirts or pants. NO bare midriffs, NO tank tops, your shirt must have sleeves and no dangly jewelry, hoodie pulls or anything else that may pose a risk of getting into the chemicals.You will not be allowed in lab if you are not properly dressed and will receive a zero for that day.

Note: as of the beginning of the semester, Husson University requires masking in all indoor buildings. If our COVID numbers decrease such that we are not required to wear masks, you should know that masks will be required in this class all semester. This decision is to protect all unvaccinated students and to provide consistency in the class. 

Failure to do so will result in removal from class with an unexcused absence.  

Tentative Schedule of Assignments

Week Tues Wednesday, Thursday
1 Safety/Checkin/Intro to Spartan Safety/Checkin/Intro to Spartan
2 IR IR
3 pKa pKa
4 NMR NMR
5 Experiment 2/3 Experiment 2/3
6 Experiment 10 Experiment 10
7 Fall Break - no lab Experiment 6, part 1
8 Experiment 6, part 1 Experiment 6, part 2
9 Experiment 6, part 2 Experiment 4, part 1
10 Experiment 4, part 1 Experiment 4, part 2
11 Experiment 4, part 2 Experiment 5, part 1
12 Experiment 5, part 1 Experiment 5, part 2
13 Experiment 5, part 2 Thanksgiving - no class
14 Nylon Nylon
15 Final exam Final exam

 

Course Summary:

Date Details Due